(2-Nitro-4-pyrrol-1-yl-phenyl)-carbamic acid tert-butyl ester → (2-Amino-4-pyrrol-1-yl-phenyl)-carbamic acid tert-butyl ester
Reaktionsgleichung
[C:1]([O:5][C:6](=[O:22])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([N:14]2[CH:18]=[CH:17][CH:16]=[CH:15]2)=[CH:10][C:9]=1[N+:19]([O-])=O)([CH3:4])([CH3:3])[CH3:2]>[Pd]>[C:1]([O:5][C:6](=[O:22])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([N:14]2[CH:15]=[CH:16][CH:17]=[CH:18]2)=[CH:10][C:9]=1[NH2:19])([CH3:4])([CH3:2])[CH3:3]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The title compound was prepared from (2-nitro-4-pyrrol-1-yl-phenyl)-carbamic acid tert-butyl ester (Example A11) by hydrogenation with 5% Pd/C according to the general procedure J (method a). Obtained as a white solid (9.06 g).
Quellen und Nachweise
- ORD-Eintrag
- ord-b131bdfd778344a88e8cb7cbb4fe434a
- Quelldatensatz
- uspto-grants-2005_09
- Patentnummer
- US06949542B2
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