Ammonia → HCID 178512765, Verbindung

HRID 49934

Reaktionsgleichung

Reaktionsgleichung von HRID 49934
[NH2:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1.N.[N:13]#[C:14][NH2:15]>O>[NH:1]([CH2:2][C:3]1[CH:4]=[CH:5][C:6]([C:7]([OH:9])=[O:8])=[CH:10][CH:11]=1)[C:14]([NH2:15])=[NH:13]

Komponenten

5

Edukt 3

HCID 222AmmoniaHCID 9864CyanamideHCID 655264-(Aminomethyl)Benzoic Acid

Produkt 1

HCID 178512765HCID 178512765, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Reaktionsbedingungen

Temperatur
60 °C

Versuchsvorschrift

A mixture of 1.51 g (10.0 mmol) of 4-aminomethylbenzoic acid, 20 ml of water, 2.0 ml of 28% aqueous ammonia and 1.00 g (23.8 mmol) of cyanamide was stirred at 60° C. overnight. The white precipitate thus formed was taken by the filtration, washed with water and dried to obtain the title compound.

Aufarbeitung

  1. customThe white precipitate thus formed
  2. filtrationwas taken by the filtration
  3. washwashed with water
  4. customdried

Quellen und Nachweise

ORD-Eintrag
ord-c887df8de4df4a55a09c1569fe4de64f
Quelldatensatz
uspto-grants-2004_03
Patentnummer
US06710056B2

Verknüpfte Notizen

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