Ammonia → 4-Amino-3,5-dichlorobenzotrifluoride
Reaktionsgleichung
[Cl:1][C:2]1[CH:3]=[C:4]([C:10]([F:13])([F:12])[F:11])[CH:5]=[C:6]([Cl:9])[C:7]=1Cl.[NH3:14]>O>[Cl:1][C:2]1[CH:3]=[C:4]([C:10]([F:13])([F:12])[F:11])[CH:5]=[C:6]([Cl:9])[C:7]=1[NH2:14]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Into a 1000 ml high-pressure reaction vessel add 200 g 3,4,5-Trichlorobenzotrifluoride and 145 g water, enclose the reaction vessel, fill liquid ammonia 380 g, close the valve, start agitation, slowly increase temperature to 160° C. and pressure to 10.0 MPa, make timed temperature-retention under controlled temperature 165° C. and controlled pressure 11.5 MPa for 8 h, then release the pressure and discharge ammonia.
Aufarbeitung
- customInto a 1000 ml high-pressure reaction vessel
- customclose the valve
- customto 160° C.
- customunder controlled temperature 165° C. and controlled pressure 11.5 MPa
- customfor 8 h
Quellen und Nachweise
- ORD-Eintrag
- ord-52f2556c81fd4dacbea8a61b3f3d9cef
- Quelldatensatz
- uspto-grants-2010_08
- Patentnummer
- US07777079B2
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