StartseiteMCPWorkbenchSkills
StartseiteWorkbenchBenachrichtigungenMein Bereich
llms.txt · MCP-AnleitungDatenschutz · Nutzungsbedingungen · Supportv1.8.0
  1. Startseite
  2. /Reaktion

Benzoyl Peroxide → Dodecyl methacrylate 2-ethylhexyl methacrylate 2-ethylhexyl acrylate

HRID 522460
Notizen
Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 522460
[C:1]([O:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:19]([O:24][CH2:25][CH:26]([CH2:31][CH3:32])[CH2:27][CH2:28][CH2:29][CH3:30])(=[O:23])[C:20]([CH3:22])=[CH2:21].[C:33]([O:37][CH2:38][CH:39]([CH2:44][CH3:45])[CH2:40][CH2:41][CH2:42][CH3:43])(=[O:36])[CH:34]=[CH2:35].C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C1CCCCC1.C(OCC)(=O)C>[C:1]([O:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:19]([O:24][CH2:25][CH:26]([CH2:31][CH3:32])[CH2:27][CH2:28][CH2:29][CH3:30])(=[O:23])[C:20]([CH3:22])=[CH2:21].[C:33]([O:37][CH2:38][CH:39]([CH2:44][CH3:45])[CH2:40][CH2:41][CH2:42][CH3:43])(=[O:36])[CH:34]=[CH2:35]
KomponentenReaktionsbedingungenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion

Komponenten

7

Edukt 4

HCID 7187Benzoyl PeroxideHCID 76362-Ethylhexyl acrylateHCID 8906Lauryl MethacrylateHCID 127132-Ethylhexyl methacrylate

Produkt 1

HCID 86729957Dodecyl methacrylate 2-ethylhexyl methacrylate 2-ethylhexyl acrylate

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 8078
Cyclohexane
Lösungsmittel
HCID 8857Ethyl AcetateLösungsmittel2×

Reaktionsbedingungen

Temperatur
80 °C

Versuchsvorschrift

An acrylic adhesive A was prepared in the following manner. A reaction liquid containing monomers including 13 parts by weight of dodecyl methacrylate, 78 parts by weight of 2-ethylhexyl methacrylate, and 9 parts by weight of 2-ethylhexyl acrylate, and 50 parts by weight of ethyl acetate was supplied to a 40-L polymerization apparatus. Subsequently, a nitrogen atmosphere at 80° C. was maintained in the polymerization apparatus. To the reaction liquid, a polymerization initiator solution prepared by dissolving 0.5 parts by weight of benzoyl peroxide in 50 parts by weight of cyclohexane was added over 24 hours to copolymerize the above monomers. After the completion of the polymerization, ethyl acetate was further added to the reaction liquid to obtain an acrylic adhesive solution A containing 35% by weight of the acrylic adhesive A including a dodecyl methacrylate/2-ethylhexyl methacrylate/2-ethylhexyl acrylate copolymer.

Aufarbeitung

  1. customAn acrylic adhesive A was prepared in the following manner
  2. customA reaction liquid
  3. additioncontaining monomers
  4. customTo the reaction liquid
  5. customa polymerization initiator solution prepared
  6. additionwas added over 24 hours to copolymerize the above monomers
  7. additionwas further added to the reaction liquid

Quellen und Nachweise

ORD-Eintrag
ord-10134d1523fc427c880519c5679af08d
Quelldatensatz
uspto-grants-2016_05
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US09333182B2

Notizen zur Reaktion

Wird geladen…

Auf dieser SeiteKomponentenReaktionsbedingungenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion