Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Acetic Acid | HCID 176 | — |
| Edukt | Benzylamine | HCID 7504 | — |
| Produkt | N-Benzylacetamide | HCID 11500 | — |
Reaktionsschritte
Benzylamine (1 mL) and acetic acid (20 mL) may be mixed together. The mixture may be heated at 115° C. for 17 hours. The excess acetic acid may be distilled from the reaction mixture using a rotary evaporator. The product may be crystallized from toluene. The mixture may be cooled to 0° C. and then filtered.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US08865920B2 |
|---|
| Quelldatensatz | uspto-grants-2014_10 |
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| ORD ID | ord-27a2c44870504edb8d0db479262b468b |
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| Quellennotiz | uspto-grants-2014_10 |
|---|