反应详情

温度

115 °C

Benzylamine (1 mL) and acetic acid (20 mL) may be mixed together. The mixture may be heated at 115° C. for 17 hours. The excess acetic acid may be distilled from the reaction mixture using a rotary evaporator. The product may be crystallized from toluene. The mixture may be cooled to 0° C. and then filtered.

1. distillationThe excess acetic acid may be distilled from the reaction mixture
2. customa rotary evaporator
3. customThe product may be crystallized from toluene
4. temperatureThe mixture may be cooled to 0° C.
5. filtrationfiltered