2-Propenoic acid, 3-hydroxypropyl ester → Isopropenylphosphonic Acid Hydroxypropylacrylate

HRID 543455

Reaktionsgleichung

Reaktionsgleichung von HRID 543455
[C:1]([P:4](=[O:7])([OH:6])[OH:5])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]>O>[C:1]([P:4](=[O:5])([OH:7])[OH:6])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]

Komponenten

4

Edukt 2

HCID 331012-Propenoic acid, 3-hydroxypropyl esterHCID 557541Isopropenylphosphonic acid

Produkt 1

HCID 86739384Isopropenylphosphonic Acid Hydroxypropylacrylate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Used the method of Example 5, isopropenyl phosphonic acid (30.7 g, 54%, 0.14 mole), hydroxypropylacrylate (36.4 g, 0.28 mole) and water (144.9 g) were charged in the reactor. The bulk of the polymer crystallized during the first period of reflux and was found to be insoluble in water.

Aufarbeitung

  1. customThe bulk of the polymer crystallized during the first period
  2. temperatureof reflux

Quellen und Nachweise

ORD-Eintrag
ord-49e0e65a7ace49c29f56fbb104f02e73
Quelldatensatz
uspto-grants-1984_05
Patentnummer
US04446028

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