HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Bromoacetonitrile → [4-(3-Methoxy-propyl)-piperazin-1-yl]acetonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Bromoacetonitrile | HCID 11534 | — |
| Edukt | 1-(3-Methoxypropyl)piperazine | HCID 1822536 | — |
| Produkt | [4-(3-Methoxy-propyl)-piperazin-1-yl]acetonitrile | HCID 63337188 | — |
Reaktionsschritte
The title compound is synthesized by coupling of 1-(3-Methoxy-propyl)-piperazine (commercially available from CHESS GmbH) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=198.2: 1HNMR(DMSO-d6) 3.65 (s, 2H), 3.30 (s, 3H), 2.45-2.20 (m, 12H), 1.65-1.55 (m, 2H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08053457B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-5a961d53f151413babf4cc3829fa4668 |
| Quellennotiz | uspto-grants-2011_11 |