HRID555735

反应详情

EQUATION

反应方程式

HRID 555735 的结构方程式

PROCEDURE

实验过程

The title compound is synthesized by coupling of 1-(3-Methoxy-propyl)-piperazine (commercially available from CHESS GmbH) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=198.2: 1HNMR(DMSO-d6) 3.65 (s, 2H), 3.30 (s, 3H), 2.45-2.20 (m, 12H), 1.65-1.55 (m, 2H).

WORKUP

后处理

  1. customanalogously to the preparation of Intermediate 149.2 as a colorless oil