Ammonium Hydroxide → 5-bromo-2-methylbenzenesulfonamide
Reaktionsgleichung
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH3:12])=[C:6]([S:8](Cl)(=[O:10])=[O:9])[CH:7]=1.[OH-].[NH4+:14]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH3:12])=[C:6]([S:8]([NH2:14])(=[O:10])=[O:9])[CH:7]=1Komponenten
3
Versuchsvorschrift
Prepared by general procedure III from 5-Bromo-2-methyl-benzenesulfonyl chloride (1.89 g, 7 mmol) and ammonium hydroxide (20 mL) to give the title compound (0.96 g, 55%) as a white solid. MS (ISN) 248.0 [(M−H)−], 250.0 [(M+2−H)−].
Quellen und Nachweise
- ORD-Eintrag
- ord-c0470a0ce5964e4cb179cac8b3d39ac8
- Quelldatensatz
- uspto-grants-2011_11
- Patentnummer
- US08063048B2
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