Dimethyl Sulfone → HCID 66727152, Verbindung

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Reaktionsgleichung

Br[C:2]1[CH:7]=[C:6]([C:8](=[O:11])[CH2:9][CH3:10])[CH:5]=[CH:4][N:3]=1.[CH3:12][S:13](C)(=[O:15])=[O:14]>>[CH3:12][S:13]([C:2]1[CH:7]=[C:6]([C:8](=[O:11])[CH2:9][CH3:10])[CH:5]=[CH:4][N:3]=1)(=[O:15])=[O:14]

Komponenten

Edukt 2

HCID 6213Dimethyl Sulfone

HCID 592773031-(2-Bromopyridin-4-yl)propan-1-one

Produkt 1

HCID 66727152HCID 66727152, Verbindung

Versuchsvorschrift

Alternatively, (1-(2-bromo-pyridin-4-yl)-propan-1-one could be converted to the corresponding methyl sulfone via the above procedure to afford 1-(2-methanesulfonyl-pyridin-4-yl)-propan-1-one. 1-(2-Methanesulfonyl-pyridin-4-yl)-propan-1-one can be converted to the title compound by methods described in example 82.

Quellen und Nachweise

ORD-Eintrag: ord-d31c6cad048e42a1984d545941caefcc
Quelldatensatz: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08063065B2

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