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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 564290Erstellt: 25. Oktober 2026

2,6-Difluoro-3-nitrobenzoic acid → 3-Amino-2,6-difluorobenzoic acid

https://huagongshe.com/reaction/564290

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2,6-Difluoro-3-nitrobenzoic acidHCID 302629—
EduktHCID 178418361HCID 178418361—
KatalysatorHCID 178418390HCID 178418390—
LösungsmittelMethanolHCID 887—
Produkt3-Amino-2,6-difluorobenzoic acidHCID 1840535293%

Reaktionsschritte

A solution of 2,6-difluoro-3-nitrobenzoic acid and 10% palladium carbon added to 10 ml of methanol was stirred in a hydrogen atmosphere at room temperature for 2 hours. The catalyst was filtered off and then the solvent was removed under a reduced pressure to obtain the desired product (Yield: 93%) as a white solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08067638B2
Quelldatensatzuspto-grants-2011_11
ORD IDord-3341bca4d0554b49aae95f7eac297a40
Quellennotizuspto-grants-2011_11