HRID564290

反应详情

EQUATION

反应方程式

HRID 564290 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 2,6-difluoro-3-nitrobenzoic acid and 10% palladium carbon added to 10 ml of methanol was stirred in a hydrogen atmosphere at room temperature for 2 hours. The catalyst was filtered off and then the solvent was removed under a reduced pressure to obtain the desired product (Yield: 93%) as a white solid.

WORKUP

后处理

  1. filtrationThe catalyst was filtered off
  2. customthe solvent was removed under a reduced pressure