Methyl 1H-indole-2-carboxylate → Methyl N-methylindole-6-carboxylate

HRID 564971

Reaktionsgleichung

Reaktionsgleichung von HRID 564971
ICCC[CH2:5][O:6][CH:7]1[CH2:12][CH2:11][CH2:10][CH2:9][O:8]1.ClC1C=CC=[C:19]2C=1[CH:16]=[C:17](C(OCC)=O)[NH:18]2.N1C2C(=CC=CC=2)[CH:30]=[C:29]1C(OC)=O>>[CH3:19][N:18]1[C:10]2[C:9](=[CH:29][CH:30]=[C:12]([C:7]([O:6][CH3:5])=[O:8])[CH:11]=2)[CH:16]=[CH:17]1

Komponenten

4

Edukt 3

HCID 70992Methyl 1H-indole-2-carboxylateHCID 11075028Ethyl 4-chloro-1H-indole-2-carboxylateHCID 111088382-(4-iodobutoxy)tetrahydropyran

Produkt 1

HCID 639843Methyl N-methylindole-6-carboxylate

Versuchsvorschrift

The title compound was prepared in a manner similar to Reference Example 5 (23) except that 2-(4-iodobutoxy)tetrahydropyran and ethyl 4-chloro-2-indolecarboxylate was used in place of 2-(2-iodoethoxy)tetrahydropyran and methyl 2-indolecarboxylate.

Quellen und Nachweise

ORD-Eintrag
ord-96386448747c402bb752190704f3eb39
Quelldatensatz
uspto-grants-2001_01
Patentnummer
US06169107A

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