Methanethiol → HCID 14698107, Verbindung
Reaktionsgleichung
[CH3:1][SH:2].F[C:4]1[CH:18]=[CH:17][C:7]([C:8]([C:10]2[S:14][C:13](=[O:15])[NH:12][C:11]=2[CH3:16])=[O:9])=[CH:6][CH:5]=1>C(O)C>[CH3:16][C:11]1[NH:12][C:13](=[O:15])[S:14][C:10]=1[C:8](=[O:9])[C:7]1[CH:17]=[CH:18][C:4]([S:2][CH3:1])=[CH:5][CH:6]=1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Gaseus methylmercaptan is added to a solution of 5-(4-fluorobenzoyl)-4-methyl-2(3H)-thiazolone (4.7 g) in ethanol (200 ml) to saturation. The mixture is heated at 120° C. in a sealed stainless steel container for 16 hours. After cooling to ambient temperature, the mixture is evaporated to dryness. The residue is recrystallized twice from ethanol to give the title compound.
Aufarbeitung
- customthe mixture is evaporated to dryness
- customThe residue is recrystallized twice from ethanol
Quellen und Nachweise
- ORD-Eintrag
- ord-fbab24ef11c248bdad4a086061127c68
- Quelldatensatz
- uspto-grants-1988_03
- Patentnummer
- US04734422
Notizen zur Reaktion
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