Dopac → Dibutylamine

HRID 570112

Reaktionsgleichung

Reaktionsgleichung von HRID 570112
NCCC1C=CC(O)=C(O)C=1.O[C:13]1C=C2[C:16]([NH:17][CH:18]=[C:19]2[CH2:20][CH2:21]N)=[CH:15][CH:14]=1.OC1C=C(CC(O)=O)C=CC=1O.OC1C=C(C=CC=1O)CN>CO>[CH2:16]([NH:17][CH2:18][CH2:19][CH2:20][CH3:21])[CH2:15][CH2:14][CH3:13]

Komponenten

6

Edukt 4

HCID 547DopacHCID 681DopamineHCID 5202SerotoninHCID 91623Dihydroxybenzylamine

Produkt 1

HCID 8148Dibutylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

Dopamine (DA, Fluka Corporation); 5-hydroxyl tryptamine (5-HT, Sigma Corporation); 3,4-dihydroxyl phenylacetic acid (DOPAC, Sigma Corporation); 3,4-dihydroxyl benzylamine (DHBA, Sigma Corporation); di-n-butylamine (Shanghai Chemical Works), D-8 ion pair reagent (Tianjin Chemical Co., Ltd.), methanol (Guaranteed Reagent, Beijing Chemical Works), other reagents are domestically produced and analytically pure.

Quellen und Nachweise

ORD-Eintrag
ord-47e2b3781fb945a5aed241050c5a88ba
Quelldatensatz
uspto-grants-2015_05
Patentnummer
US09023817B2

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