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Water → 1-Methyl-3-methylidenecyclobutane-1-carboxylic acid

HRID 577746
Notizen
Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 577746
[OH-:1].[K+].[CH3:3][C:4]1([C:9]#N)[CH2:7][C:6](=[CH2:8])[CH2:5]1.[OH2:11]>CCO>[CH3:3][C:4]1([C:9]([OH:11])=[O:1])[CH2:7][C:6](=[CH2:8])[CH2:5]1
KomponentenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion

Komponenten

5

Edukt 3

HCID 962WaterHCID 14797Potassium HydroxideHCID 234468681-Methyl-3-methylidenecyclobutane-1-carbonitrile

Produkt 1

HCID 206145171-Methyl-3-methylidenecyclobutane-1-carboxylic acid

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

To a solution of KOH (12.0 g, 213 mmol) in water (10 mL) and EtOH (10 mL) was added 1-methyl-3-methylidenecyclobutanecarbonitrile (53.3 mmol, crude) and the resulting solution was heated to reflux for 2.5 hrs. The mixture was cooled to rt and the solvent was removed under vacuum. The residue was diluted with water (30 mL) and washed with EtOAc (30 mL). The aqueous layer was acidified with concentrated HCl to pH˜1 in ice bath, and then extracted with EtOAc (two×30 mL). The combined organics were dried over MgSO4 and concentrated to give the title compound acid as pale brown liquid. 1H NMR (400 MHz, chloroform-d) δ ppm 4.90 (quin, J=2.41 Hz, 2H), 3.16-3.34 (m, 2H), 2.54 (qd, J=2.10, 16.57 Hz, 2H), 1.49 (s, 3H).

Aufarbeitung

  1. temperaturethe resulting solution was heated
  2. temperatureto reflux for 2.5 hrs
  3. customthe solvent was removed under vacuum
  4. additionThe residue was diluted with water (30 mL)
  5. washwashed with EtOAc (30 mL)
  6. extractionextracted with EtOAc (two×30 mL)
  7. dry with materialThe combined organics were dried over MgSO4
  8. concentrationconcentrated

Quellen und Nachweise

ORD-Eintrag
ord-2b96e0dc5cbf47b5a4b727079d5b47fa
Quelldatensatz
uspto-grants-2015_05
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US09040547B2

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