Acetone → Adipic acid di(2-propylidene hydrazide)

HRID 578615

Reaktionsgleichung

Reaktionsgleichung von HRID 578615
O.[C:2]([NH:12][NH2:13])(=[O:11])[CH2:3][CH2:4][CH2:5][CH2:6][C:7]([NH:9][NH2:10])=[O:8].C([O-])(=O)[C:15]([CH3:17])=[CH2:16].[CH3:20][C:21](=O)[CH3:22]>>[CH:16](=[N:10][NH:9][C:7](=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][C:2]([NH:12][N:13]=[CH:20][CH2:21][CH3:22])=[O:11])[CH2:15][CH3:17]

Komponenten

5

Edukt 4

HCID 180AcetoneHCID 962WaterHCID 66117Adipic DihydrazideHCID 87595Methacrylate

Produkt 1

HCID 86666342Adipic acid di(2-propylidene hydrazide)

Versuchsvorschrift

In a stainless steel flask equipped with an agitator, 45.6 grams of water were added, the agitator was turned on, then 25 grams of adipic acid dihydrazide were added. The mixture was agitated for at least 10 minutes until a stable dispersion was formed. 16.4 grams of 2-propanone were then added under mixing. A clear solution formed after a few minutes. Mixing was continued for at least another hour until reaction product precipitated and formed a stable dispersion. The temperature of the dispersion was allowed to drop to 105° F. or below, and 10 grams of an acrylic latex containing 51% of methacrylate and butyl acrylic polymer were added, followed by 3.0 grams of AQUAFLOW NLS-200. The Stormer viscosity of the dispersion was 105 Kreb units at 77° F.

Aufarbeitung

  1. additionwere added
  2. additionwere added
  3. customwas formed
  4. additionunder mixing
  5. customA clear solution formed after a few minutes
  6. additionMixing
  7. customuntil reaction product
  8. customprecipitated
  9. customformed a stable dispersion
  10. customto drop to 105° F. or below
  11. additionwere added
  12. customat 77° F.

Quellen und Nachweise

ORD-Eintrag
ord-3bf3f3bf508b43beb484128b01b184d8
Quelldatensatz
uspto-grants-2015_05
Patentnummer
US09040617B2

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