Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Decanoic Acid | HCID 2969 | — |
| Edukt | Risperidone | HCID 5073 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Risperidone Decanoate | HCID 131732870 | — |
Reaktionsschritte
150 ml of ethanol and 5 gm Risperidone were charged in the flask. The reaction mixture was heated at 50-55° C. and stirred for 10 minutes to get clear solution. 2.1 gm decanoic acid solution in 30 ml ethanol was added to the reaction mixture at 40-45° C. The reaction mixture was further cooled to 25-30° C., stirred for 18-20 hours and distilled out completely under vacuum at 50-55° C. The solid was dried under vacuum at 40-45° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US09040695B2 |
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| Quelldatensatz | uspto-grants-2015_05 |
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| ORD ID | ord-d79fd3f721be46d5aad743def91d2ae3 |
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| Quellennotiz | uspto-grants-2015_05 |
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