Dimethyl Sulfide → (2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide
Reaktionsgleichung
[Br:1][CH2:2][C:3]([O:5][CH2:6][CH3:7])=[O:4].[CH3:8][S:9][CH3:10]>CC(C)=O>[Br-:1].[C:3]([CH2:2][S+:9]([CH3:10])[CH3:8])([O:5][CH2:6][CH3:7])=[O:4]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A solution of ethyl bromoacetate (265 g) and dimethyl sulfide (114 g) in acetone (500 mL) was stirred at room temperature. After three days, the title compound was isolated by filtration of the reaction mixture. Melting point 88-90° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-950d9b632701446f88a52f5033b6d2e5
- Quelldatensatz
- uspto-grants-1999_07
- Patentnummer
- US05925782
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