Iodoethane → 4-(4-Chloro-3-trifluoromethyl-phenyl)-1-ethyl-piperidine
Reaktionsgleichung
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[C:14]([F:17])([F:16])[F:15].I[CH2:19][CH3:20]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:13][CH2:12][N:11]([CH2:19][CH3:20])[CH2:10][CH2:9]2)=[CH:4][C:3]=1[C:14]([F:17])([F:15])[F:16]Komponenten
3
Versuchsvorschrift
Beginning with 4-(4-Chloro-3-trifluoromethyl-phenyl)-piperidine and iodoethane, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 291 (M+, 6), 278 (29), 277 (11), 276 (bp), 70 (50).
Aufarbeitung
- customthe title compound was recovered by the procedure
Quellen und Nachweise
- ORD-Eintrag
- ord-f36be6d835f14255a13beaa52b0d19b0
- Quelldatensatz
- uspto-grants-2005_08
- Patentnummer
- US06924374B2
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