Morpholine → HCID 178513121, Verbindung
Reaktionsgleichung
I.[NH:2]([C:4](SC)=[NH:5])[NH2:3].[NH:8]1[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1>CO>[N:8]1([C:4](=[NH:5])[NH:2][NH2:3])[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To a solution of methyl hydrazinecarbimidothioate hydroiodide (0.100 g, 0.429 mmol) in MeOH (2 mL) was added morpholine (0.075 mL, 0.858 mmol) and refluxed overnight. Reaction was cool to RT and concentrated to get morpholine-4-carboximidhydrazide as a white solid in quantitative yield.
Aufarbeitung
- temperaturerefluxed overnight
- customReaction
- concentrationconcentrated
Quellen und Nachweise
- ORD-Eintrag
- ord-6407090cb11347459dd3c8c7f1ae4f0f
- Quelldatensatz
- uspto-grants-2016_01
- Patentnummer
- US09227971B2
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