Sulfamide → HCID 86706430, Verbindung

HRID 589957Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 589957
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].[O:6]=[S:7]1(=[O:14])[CH2:11][CH2:10][CH:9]([CH2:12]N)[CH2:8]1>O>[O:6]=[S:7]1(=[O:14])[CH2:11][CH2:10][CH:9]([CH2:12][NH:4][S:1](=[O:3])(=[O:2])[NH2:5])[CH2:8]1

Komponenten

4

Edukt 2

HCID 82267SulfamideHCID 27722253-(Aminomethyl)-1lambda~6~-thiolane-1,1-dione

Produkt 1

HCID 86706430HCID 86706430, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Sulfamide (2.4 mmol) was dissolved in H2O (10 mL), added (1,1-dioxothiolan-3-yl)methanamine (2 mmol) and stirred at reflux for 16 h. The obtained reaction mixture was cooled to rt and freezedried affording the title compound as an oil. Used without further purification.

Aufarbeitung

  1. temperatureat reflux for 16 h
  2. customThe obtained reaction mixture
  3. customfreezedried

Quellen und Nachweise

ORD-Eintrag
ord-bc55470bd0764475824846dcf93f7959
Quelldatensatz
uspto-grants-2016_01
Patentnummer
US09233964B2

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