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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 597022Erstellt: 25. Oktober 2026

2,3-Dichlorothioanisole → 2',3'-Dichloro-4'-methylthio-2-cyclopentylacetophenone

https://huagongshe.com/reaction/597022

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2,3-DichlorothioanisoleHCID 2758224—
EduktCyclopentylacetyl chlorideHCID 3485182—
EduktAluminum(III) ChlorideHCID 6451240—
LösungsmittelDichloromethaneHCID 6344—
Produkt2',3'-Dichloro-4'-methylthio-2-cyclopentylacetophenoneHCID 20358446—

Reaktionsschritte

2',3'-Dichloro-4'-methylthio-2-cyclopentylacetophenone is prepared following substantially the same procedure described in Example 3, Step A, using the following substances: 2,3-dichlorothioanisole (63.1 g., 0.327 mole), methylene chloride (300 ml.), cyclopentylacetyl chloride (52.7 g., 0.367 mole) and aluminum chloride (48.0 g., 0.36 mole).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04012524
Quelldatensatzuspto-grants-1977_03
ORD IDord-2db9715d379746e78417b853bc30eb3e
Quellennotizuspto-grants-1977_03