Sodium methanethiolate → 3,5-Dicyano-2-mercaptobenzonitrile
Reaktionsgleichung
Br[C:2]1[C:9]([C:10]#[N:11])=[CH:8][C:7]([C:12]#[N:13])=[CH:6][C:3]=1[C:4]#[N:5].C[S-:15].[Na+]>>[C:4]([C:3]1[C:2]([SH:15])=[C:9]([CH:8]=[C:7]([C:12]#[N:13])[CH:6]=1)[C:10]#[N:11])#[N:5]Komponenten
3
Versuchsvorschrift
If the procedure described in Preparation LV is followed starting from 6 g (26.10-3 mol) of 2-bromo-3,5-dicyanobenzonitrile and 6 g (86.10-3 mol) of sodium thiomethylate, 6 g (quantitative yield) of the expected product are obtained in the form of an oil.
Aufarbeitung
- customIf the procedure described in Preparation LV
Quellen und Nachweise
- ORD-Eintrag
- ord-68057794265042cf843f66f80857944b
- Quelldatensatz
- uspto-grants-1993_09
- Patentnummer
- US05246961
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