Diethylamine → HCID 13090789, Verbindung
Reaktionsgleichung
[Cl:1][C:2]1[CH:3]=[N:4][C:5]2[C:10]([CH:11]=1)=[CH:9][CH:8]=[C:7]([Cl:12])[C:6]=2[CH2:13]Cl.[CH2:15]([NH:17][CH2:18][CH3:19])[CH3:16]>O>[Cl:1][C:2]1[CH:3]=[N:4][C:5]2[C:10]([CH:11]=1)=[CH:9][CH:8]=[C:7]([Cl:12])[C:6]=2[CH2:13][N:17]([CH2:18][CH3:19])[CH2:15][CH3:16]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
24.6 parts of 3,7-dichloro-8-chloromethylquinoline and 30 parts of diethylamine were stirred at 55° C. for 6 hours. Water was added and the solid was filtered off with suction and dried. 25 parts of 3,7-dichloro-8-diethylaminomethylquinoline of melting point 54° C. were obtained. The yield corresponds to 89% of theory.
Aufarbeitung
- filtrationthe solid was filtered off with suction
- customdried
Quellen und Nachweise
- ORD-Eintrag
- ord-10d20af6330a49038d3c50d2204a5937
- Quelldatensatz
- uspto-grants-1985_02
- Patentnummer
- US04497651
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