Methyl iodide → HCID 20370471, Verbindung
Reaktionsgleichung
[CH3:1][N:2]([CH3:19])[C:3](=[O:18])[CH:4]([CH3:17])[N:5]1[CH:9]=[C:8](C)[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[N:6]1.CI.[CH2:22](I)[CH3:23]>>[CH3:19][N:2]([CH3:1])[C:3](=[O:18])[C:4]([CH3:17])([C:23]1[CH:22]=[CH:9][CH:8]=[CH:7][CH:11]=1)[N:5]1[CH:9]=[CH:8][C:7]([C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=2)=[N:6]1Komponenten
4
Versuchsvorschrift
Following the procedure of Example 95, but substituting N,N-dimethyl-α,3-diphenylpyrazole-1-acetamide for N,N,α,4-tetramethyl-3-phenylpyrazole-1-acetamide and methyl iodide for ethyl iodide, there is obtained N,N,α-trimethyl-α,3-diphenylpyrazole-1-acetamide, m.p. 129°-131.5° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-c0516e7cf19d4c18a1e19eb886b64b07