HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Chloroethyldiisopropylammonium chloride → 2-Propanamine, N-(1-methylethyl)-N-(2-(2-(2-methylpropoxy)phenoxy)ethyl)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Chloroethyldiisopropylammonium chloride | HCID 77942 | — |
| Edukt | 2-Isobutoxyphenol | HCID 691161 | — |
| Edukt | Sodium | HCID 5360545 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 2-Propanamine, N-(1-methylethyl)-N-(2-(2-(2-methylpropoxy)phenoxy)ethyl)- | HCID 3042673 | — |
Reaktionsschritte
The compound was prepared as described in Example 1, using sodium (3.45 g; 150 mmole), o-isobutoxyphenol (12.45 g; 75 mmole) and diisopropylaminoethylchloride hydrochloride (15.0 g; 75 mmole) in 200 ml of ethanol. Yield 11.2 g (51%) of product, boiling at 111°-113° C under a pressure of 0.001 mm.Hg, nD25 : 1.4920.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04073917 |
| Quelldatensatz | uspto-grants-1978_02 |
| ORD ID | ord-d9826df901224041ac2bf5f085253604 |
| Quellennotiz | uspto-grants-1978_02 |