HRID616372

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID77942

N-(2-chloroethyl)-N-(propan-2-yl)propan-2-amine hydrochloride

C8H19Cl2N

HCID691161

2-isobutoxyphenol

C10H14O2

HCID5360545

Sodium

PRODUCTS

生成物

HCID3042673

2-Propanamine, N-(1-methylethyl)-N-(2-(2-(2-methylpropoxy)phenoxy)ethyl)-

C18H31NO2

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

The compound was prepared as described in Example 1, using sodium (3.45 g; 150 mmole), o-isobutoxyphenol (12.45 g; 75 mmole) and diisopropylaminoethylchloride hydrochloride (15.0 g; 75 mmole) in 200 ml of ethanol. Yield 11.2 g (51%) of product, boiling at 111°-113° C under a pressure of 0.001 mm.Hg, nD25 : 1.4920.

WORKUP

后处理

customThe compound was prepared