Acetonitrile → Disodium adipate

HRID 616621

Reaktionsgleichung

Reaktionsgleichung von HRID 616621
[C:1]([O:11]C)(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=[O:7].C(#N)C.[OH-].[Na+:17]>O>[C:1]([O-:11])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:17].[Na+:17]

Komponenten

5

Edukt 3

HCID 6342AcetonitrileHCID 12329DimethyladipateHCID 14798Sodium Hydroxide

Produkt 1

HCID 24073Disodium adipate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

17.4 Grams (0.1 mole) of dimethyl adipate are dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 Grams (0.2 mole) of sodium hydroxide dissolved in 6.0 g. of water are added to the reaction mixture. The reaction mixture is stirred at reflux temperature for 18 hours. The resulting solution is filtered hot and the solids are air dried to yield disodium adipate as the reaction product.

Aufarbeitung

  1. temperatureat reflux temperature for 18 hours
  2. filtrationThe resulting solution is filtered hot
  3. customdried

Quellen und Nachweise

ORD-Eintrag
ord-4a44ab5cc5df4d7eaf36af8930e8ae52
Quelldatensatz
uspto-grants-1978_02
Patentnummer
US04075234

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