Hydrochloric Acid → 3-Methoxyiminopyrrolidine hydrochloride
Reaktionsgleichung
[ClH:1].C(OC([N:9]1[CH2:13][CH2:12][C:11](=[N:14][O:15][CH3:16])[CH2:10]1)=O)(C)(C)C.CCOCC>C(OCC)(=O)C>[ClH:1].[CH3:16][O:15][N:14]=[C:11]1[CH2:12][CH2:13][NH:9][CH2:10]1Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Reaktionsbedingungen
- Temperatur
- 40 °C
Versuchsvorschrift
7 ml of a 3M hydrogen chloride solution in ethyl acetate was added to 2.3 g of ice-cooled 1-(t-butoxycarbonyl)-3-methoxyiminopyrrolidine, and the mixture was stirred at about 40° C. for one hour. After completion of the reaction, the solvent was stripped off from the reaction mixture and ether was added to the residue. The crystals which formed were collected by filtration and washed with ether, giving 1.5 g of the title compound.
Aufarbeitung
- customAfter completion of the reaction
- additionwas added to the residue
- customThe crystals which formed
- filtrationwere collected by filtration
- washwashed with ether
Quellen und Nachweise
- ORD-Eintrag
- ord-717408610b5640e58a55825510da26e4
- Quelldatensatz
- uspto-grants-1988_09
- Patentnummer
- US04771046
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