Thiophenol → Diphenyl sulfide

HRID 623238

Reaktionsgleichung

Reaktionsgleichung von HRID 623238
[C:1]1([SH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>C1(C)C=CC=CC=1>[C:1]1([S:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Komponenten

3

Edukt 1

HCID 7969Thiophenol

Produkt 1

HCID 8766Diphenyl sulfide

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

A mixture of bis(dineophyl-orthotrifluoromethylphenyltin)oxide (6.0 g, 5.6 mmol) prepared in Example 6, thiophenol (1.2 g, 11.2 mmol) and toluene (40 g) was treated with the procedure described in Example 7. The product was recrystallized from n-hexane to obtain 5.2 g of dineophylorthotrifluoromethylphenyltin phenylsulfide as a white solid.

Aufarbeitung

  1. additionwas treated with the procedure
  2. customThe product was recrystallized from n-hexane

Quellen und Nachweise

ORD-Eintrag
ord-7087eac787814b4481a45eda5fa3f06b
Quelldatensatz
uspto-grants-1988_09
Patentnummer
US04774235

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