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3-Methylcatechol → Catechol

HRID 647607
Notizen
Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 647607
[CH3:1][C:2]1[CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[C:3]=1[OH:9].C1(C)C=CC=CC=1>C1C=CC=CC=1>[CH3:1][C:2]1[CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[C:3]=1[OH:9].[C:4]1([C:3](=[CH:2][CH:8]=[CH:7][CH:6]=1)[OH:9])[OH:5].[C:2]1([CH3:1])[C:3]([OH:9])=[CH:4][CH:6]=[CH:7][CH:8]=1.[C:4]1([OH:5])[CH:6]=[CH:7][CH:8]=[CH:2][CH:3]=1
KomponentenReaktionsbedingungenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion

Komponenten

7

Edukt 2

HCID 3403-MethylcatecholHCID 1140Toluene

Produkt 4

HCID 289CatecholHCID 335O-CresolHCID 3403-MethylcatecholHCID 996Phenol

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 241
Benzene
Lösungsmittel

Reaktionsbedingungen

Temperatur
1600 fahrenheit

Versuchsvorschrift

The effluent crackate vapor is separated from particulate solids in a cyclone separator, and the solids containing coke deposits are passed into the upper end of an ordinary or slow fluidized bed combustion zone maintained at about 1600° F. temperature for combustion of coke. Heated air and superheated steam are introduced into the lower end of the slow fluidized bed combustion zone. The hot decoked solids are recycled to the lower end of the fast fluidized bed, and flue gas is withdrawn from the top of the slow bed. The typical product slate that is obtained if secondary reactions are minimized is given in Table 1, with methyl catechol being the principal product. Increased process severity produces more secondary conversion of methyl catechol to catechol, cresol, phenol, toluene, and benzene. In addition, some tar is formed.

Aufarbeitung

  1. customThe effluent crackate vapor is separated from particulate solids in a cyclone separator
  2. additionthe solids containing coke deposits
  3. temperatureHeated air and superheated steam
  4. additionare introduced into the lower end of the
  5. customis withdrawn from the top of the slow bed
  6. customThe typical product slate that is obtained if secondary reactions
  7. temperatureIncreased process severity

Quellen und Nachweise

ORD-Eintrag
ord-d8d7b7e410d84b4eb69ff00655c41ef3
Quelldatensatz
uspto-grants-1983_10
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US04409416

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