Cesium fluoride → Allyl Oxalofluoride

HRID 649255Notizen

Reaktionsgleichung

[CH2:1]([O:4][C:5](=[O:9])[C:6](Cl)=[O:7])[CH:2]=[CH2:3].[F-:10].[Cs+]>>[CH2:1]([O:4][C:5](=[O:9])[C:6]([F:10])=[O:7])[CH:2]=[CH2:3]

Komponenten

Edukt 2

HCID 25953Cesium fluoride

HCID 3018516Allyl chlorooxoacetate

Produkt 1

HCID 14153244Allyl Oxalofluoride

Versuchsvorschrift

By the procedure of the preceding Preparation, allyl oxalochloride (252.5 g, 1.70 mol) and cesium fluoride (284 g, 1.87 mol) were converted to twice distilled title product, b.p. 48°-50° C./35 mm; 124°-126° C. (atmospheric pressure).

Aufarbeitung

distillationto twice distilled title product, b.p. 48°-50° C./35 mm
custom124°-126° C. (atmospheric pressure)

Quellen und Nachweise

ORD-Eintrag: ord-e0232b6b3e3e495ca8bd281a4b73c66e
Quelldatensatz: uspto-grants-1988_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04739047

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