Hydrochloric Acid → Benzenediazonium chloride

HRID 65551

Reaktionsgleichung

Reaktionsgleichung von HRID 65551
[ClH:1].[NH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.Cl.[N:10]([O-])=O.[Na+]>O>[Cl-:1].[C:3]1([N+:2]#[N:10])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 8870Benzenamine hydrochloride (1:1)HCID 23668193Sodium Nitrite

Produkt 1

HCID 60992Benzenediazonium chloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel2×

Versuchsvorschrift

A solution of benzenediazonium chloride was prepared as follows: To an ice cold (about 5° C.) solution of aniline hydrochloride (3.24 g., 25 mmoles) in water (10 ml.) and concentrated hydrochloric acid (2.1 ml., 25 mmoles) was added dropwise with stirring a solution of sodium nitrite (1.9 g., 27.5 mmoles) in water (10 ml.). After addition the solution was stirred in the cold for an additional 15 minutes.

Aufarbeitung

  1. additionAfter addition the solution

Quellen und Nachweise

ORD-Eintrag
ord-9a32150a3bf545fe94a430c25ee8ca32
Quelldatensatz
uspto-grants-1978_12
Patentnummer
US04128425

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