Propylenediamine → HCID 178442710, Verbindung
Reaktionsgleichung
[NH2:1][CH2:2][CH:3]([NH2:5])[CH3:4].[C:6](O)(=O)[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>>[CH3:4][CH:3]1[CH2:2][NH:1][C:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])=[N:5]1Komponenten
3
Reaktionsbedingungen
- Temperatur
- 170 °C
Versuchsvorschrift
1,2-Diaminopropane 61.5 g (0.7 mole) was delivered to a reaction vessel and pelargonic acid 112 g (0.7 mole) was added slowly. The mixture was slowly heated to 170° C. while removing water of reaction. There was obtained 4-methyl-2-octyl-2-imidazoline. To it was added 42 g of paraformaldehyde with stirring. The mixture was heated to about 100° C. for 3 hours to produce N1 -hydroxymethyl-4-methyl-2-octyl-2-imidazoline.
Aufarbeitung
- customwhile removing
- customwater of reaction