Orotic Acid → Creatine orotate

HRID 657439

Reaktionsgleichung

Reaktionsgleichung von HRID 657439
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1>C(O)C>[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]

Komponenten

4

Edukt 2

HCID 967Orotic AcidHCID 80116Creatine Monohydrate

Produkt 1

HCID 12135009Creatine orotate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Under room temperature 149 grams of creatine monohydrate is slowly added to 1.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with ethanol. After drying 272 grams of creatine orotate is obtained.

Aufarbeitung

  1. stirringduring continuous stirring for 4 hours under room temperature
  2. filtrationFinally filtration
  3. customto remove the solvent
  4. dry with materialAfter drying 272 grams of creatine orotate
  5. customis obtained

Quellen und Nachweise

ORD-Eintrag
ord-90a9bcc616464073b559974dbcdb47a5
Quelldatensatz
uspto-grants-2011_12
Patentnummer
USRE043029E1

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