Orotic Acid → Dicreatine orotate

HRID 657440

Reaktionsgleichung

Reaktionsgleichung von HRID 657440
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1>C(O)C>[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]

Komponenten

4

Edukt 2

HCID 967Orotic AcidHCID 80116Creatine Monohydrate

Produkt 1

HCID 131724698Dicreatine orotate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Under room temperature 298 grams of creatine monohydrate is slowly added to 2.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with ethanol. After drying 410 grams of Dicreatine orotate is obtained.

Aufarbeitung

  1. stirringduring continuous stirring for 4 hours under room temperature
  2. filtrationFinally filtration
  3. customto remove the solvent
  4. dry with materialAfter drying 410 grams of Dicreatine orotate
  5. customis obtained

Quellen und Nachweise

ORD-Eintrag
ord-bf3c6f5643184be7a9652d70df81c39a
Quelldatensatz
uspto-grants-2011_12
Patentnummer
USRE043029E1

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