Orotic Acid → Tricreatine orotate

HRID 657441

Reaktionsgleichung

Reaktionsgleichung von HRID 657441
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1>C(O)C>[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]

Komponenten

4

Edukt 2

HCID 967Orotic AcidHCID 80116Creatine Monohydrate

Produkt 1

HCID 11444210Tricreatine orotate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Under room temperature 447 grams of creatine monohydrate is slowly added to 3.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with alcohol. After drying 555 grams of Tricreatine orotate is obtained.

Aufarbeitung

  1. stirringduring continuous stirring for 4 hours under room temperature
  2. filtrationFinally filtration
  3. customto remove the solvent
  4. dry with materialAfter drying 555 grams of Tricreatine orotate
  5. customis obtained

Quellen und Nachweise

ORD-Eintrag
ord-9e2a2e1f8b6146c28c4ae7c7957b50e8
Quelldatensatz
uspto-grants-2011_12
Patentnummer
USRE043029E1

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