Dimethyladipate → Disodium adipate

HRID 65824

Reaktionsgleichung

Reaktionsgleichung von HRID 65824
[C:1]([O:11]C)(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=[O:7].[OH-].[Na+:14]>C(#N)C>[C:1]([O-:11])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:14].[Na+:14]

Komponenten

4

Edukt 2

HCID 12329DimethyladipateHCID 14798Sodium Hydroxide

Produkt 1

HCID 24073Disodium adipate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6342AcetonitrileLösungsmittel

Versuchsvorschrift

17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.

Aufarbeitung

  1. temperatureat reflux temperature for 18 hours
  2. filtrationThe resulting solution was filtered hot
  3. customdried

Quellen und Nachweise

ORD-Eintrag
ord-af3c1eef92454c249d5f397014b710cf
Quelldatensatz
uspto-grants-1978_12
Patentnummer
US04129520

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