Dimethyladipate → Disodium adipate
Reaktionsgleichung
[C:1]([O:11]C)(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=[O:7].[OH-].[Na+:14]>C(#N)C>[C:1]([O-:11])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:14].[Na+:14]Komponenten
4
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.
Aufarbeitung
- temperatureat reflux temperature for 18 hours
- filtrationThe resulting solution was filtered hot
- customdried
Quellen und Nachweise
- ORD-Eintrag
- ord-af3c1eef92454c249d5f397014b710cf
- Quelldatensatz
- uspto-grants-1978_12
- Patentnummer
- US04129520
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