HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
9,10-Dimethylanthracene → Anthracene, 9,10-dihydro-9,10-dimethyl-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 9,10-Dimethylanthracene | HCID 13076 | — |
| Katalysator | HCID 178505374 | HCID 178505374 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | Anthracene, 9,10-dihydro-9,10-dimethyl- | HCID 606352 | 8% |
Reaktionsschritte
9,10-Dihydro-9,10-dimethylanthracene was prepared by hydrogenation of 9,10-dimethylanthracene with Girdler G-22 copper chromite catalyst in toluene at 120° C. and 1500 psi for 1 hour. The mixtures resulting from five such runs were combined and filtered, and the off-white solid product was isolated by evaporating the solvent. It was characterized by nmr spectroscopy.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04131646 |
| Quelldatensatz | uspto-grants-1978_12 |
| ORD ID | ord-33838fd7755847479484c70ff8d9c312 |
| Quellennotiz | uspto-grants-1978_12 |