4-Bromoaniline → 2-(4-bromophenyl)-6-butoxy-3,4-dihydro-2H-isoquinolin-1-one

HRID 69456

Reaktionsgleichung

Reaktionsgleichung von HRID 69456
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH2:8])=[CH:4][CH:3]=1.[CH2:9]([O:13][C:14]1[CH:22]=[CH:21][C:17]([C:18](Cl)=[O:19])=[C:16]([CH2:23][CH2:24]Cl)[CH:15]=1)[CH2:10][CH2:11][CH3:12]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:24][CH2:23][C:16]3[C:17](=[CH:21][CH:22]=[C:14]([O:13][CH2:9][CH2:10][CH2:11][CH3:12])[CH:15]=3)[C:18]2=[O:19])=[CH:4][CH:3]=1

Komponenten

3

Edukt 2

HCID 78074-BromoanilineHCID 534401334-Butoxy-2-(2-chloroethyl)benzoyl chloride

Produkt 1

HCID 689911152-(4-bromophenyl)-6-butoxy-3,4-dihydro-2H-isoquinolin-1-one

Versuchsvorschrift

According to Method A, 4-bromo-phenylamine was reacted with 4-butoxy-2-(2-chloroethyl)-benzoyl chloride. In this way the product was obtained with molecular weight 374.28 (C19H20BrNO2); MS (ESI): 374 (M+H+).

Aufarbeitung

  1. customIn this way the product was obtained with molecular weight 374.28 (C19H20BrNO2)

Quellen und Nachweise

ORD-Eintrag
ord-0ce0a7a5fbc149c4a58b526ad48469b4
Quelldatensatz
uspto-grants-2014_09
Patentnummer
US08822495B2

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