Cyanuric chloride → 1,3,5-Triazine, 2,4,6-tris(1-azetidinyl)-

HRID 704114Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 704114
[NH:1]1[CH2:4][CH2:3][CH2:2]1.[N:5]1[C:12](Cl)=[N:11][C:9](Cl)=[N:8][C:6]=1Cl>O>[N:1]1([C:6]2[N:8]=[C:9]([N:1]3[CH2:4][CH2:3][CH2:2]3)[N:11]=[C:12]([N:1]3[CH2:4][CH2:3][CH2:2]3)[N:5]=2)[CH2:4][CH2:3][CH2:2]1

Komponenten

4

Edukt 2

HCID 7954Cyanuric chlorideHCID 10422Azetidine

Produkt 1

HCID 1520761,3,5-Triazine, 2,4,6-tris(1-azetidinyl)-Ausbeute 78 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Compound LXXVI was prepared after the method of Schaefer (J Am Chem Soc (1955) 77 p592B). The hydrochloride salt of azetidine was reacted with cyanuric chloride in water to give compound LXXVI as a white solid (yield 78%) having a melting point of 225°-238° C. The 1Hnmr of this compound indicated that its identity was correct and that its purity was adequate for subsequent reactions without further purification.

Aufarbeitung

  1. customCompound LXXVI was prepared after the method of Schaefer (J Am Chem Soc (1955) 77 p592B)

Quellen und Nachweise

ORD-Eintrag
ord-5e35f850284549238e6e160ccc3f5f5b
Quelldatensatz
uspto-grants-1991_01
Patentnummer
US04985584

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