Methacrylic Acid → Solanone

HRID 716607Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 716607
C(O)(=O)C(C)=C.CC(C(OCCOC(C(C)=C)=O)=O)=C.[CH:21]([CH:24]([CH2:30][CH2:31][CH:32]([CH3:34])[CH3:33])[CH2:25][CH2:26][C:27](=[O:29])[CH3:28])([CH3:23])[CH3:22]>C1(C)C=CC=CC=1>[CH3:23][CH:21]([C@@H:24](/[CH:30]=[CH:31]/[C:32]([CH3:34])=[CH2:33])[CH2:25][CH2:26][C:27]([CH3:28])=[O:29])[CH3:22]

Komponenten

5

Edukt 3

HCID 4093Methacrylic AcidHCID 7355Ethylene glycol dimethacrylateHCID 89183541HCID 89183541, Verbindung

Produkt 1

HCID 6451337Solanone

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

Methacrylic acid (3 mol percent), EGDMA (95 mol percent), and 5-isopropyl-8-methylnonan-2-one (2 mol percent) are combined in toluene. 2,2-Azobisisobutyronitrile (AIBN) is added as an initiator. The reaction flask is degassed, purged with dry nitrogen, and sealed. The solution is irradiated with a UV lamp (365 nm) to activate the AIBN and initiate the polymerization reaction.

Aufarbeitung

  1. customThe reaction flask is degassed
  2. custompurged with dry nitrogen
  3. customsealed
  4. customThe solution is irradiated with a UV lamp (365 nm)
  5. customthe polymerization reaction

Quellen und Nachweise

ORD-Eintrag
ord-b5ac5cf49dcf4455a1dc12b61b82caa9
Quelldatensatz
uspto-grants-2015_11
Patentnummer
US09192193B2

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