Diethyl Ether → HCID 22597223, Verbindung

HRID 7193

Reaktionsgleichung

Reaktionsgleichung von HRID 7193
[CH3:1][C:2]1(O)[CH:9]2[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:11][CH:3]1[CH2:4]3)[CH2:8]2.[C:13](Cl)(=[O:16])[CH:14]=[CH2:15].C([O:20]CC)C>>[C:13]([O:16][C:3]12[CH2:11][CH:7]3[CH2:6][CH:5]([CH2:10][CH:9]([CH2:8]3)[CH:2]1[CH3:1])[CH2:4]2)(=[O:20])[CH:14]=[CH2:15]

Komponenten

4

Edukt 3

HCID 3283Diethyl EtherHCID 13140Acryloyl chlorideHCID 1365452-Methyl-2-adamantanol

Produkt 1

HCID 22597223HCID 22597223, VerbindungAusbeute 55 %

Versuchsvorschrift

200 mL of diethyl ether was put into a round-neck flask, 41.5 g of 2-methyl-2-adamantanol and 27.6 g of tetraethyl amine were added thereto and then 22.6 g of acryloyl chloride was dropped. The reactant was reacted at room temperature for about 12 hours and then filtered using diethyl ether. Subsequently, the solvent was removed by an evaporator and then the reactant product was obtained using vacuum distillation (yield: 55%).

Aufarbeitung

  1. customThe reactant was reacted at room temperature for about 12 hours
  2. filtrationfiltered
  3. customSubsequently, the solvent was removed by an evaporator
  4. customthe reactant product was obtained
  5. distillationvacuum distillation (yield: 55%)

Quellen und Nachweise

ORD-Eintrag
ord-36f2de1457284bf3b0fda06e472eab7b
Quelldatensatz
uspto-grants-2006_08
Patentnummer
US07084227B2

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