HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyanogen Bromide → 5-(2-Nitrophenyl)-1,3,4-oxadiazol-2-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyanogen Bromide | HCID 10476 | — |
| Edukt | o-Nitrobenzohydrazide | HCID 3781218 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 5-(2-Nitrophenyl)-1,3,4-oxadiazol-2-amine | HCID 712042 | — |
Reaktionsschritte
4 ml of a 5M cyanogen bromide solution in acetonitrile were added dropwise to the solution of 3.6 g of 2-nitrobenzoic hydrazide in 20 ml of acetonitrile. This resulted first in a clear solution, then a solid precipitated out which was filtered off with suction after continuing to stir for a short time, washed again with acetonitrile and dried under reduced pressure.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07138414B2 |
| Quelldatensatz | uspto-grants-2006_11 |
| ORD ID | ord-db67281e842a443a941f216a9cc75985 |
| Quellennotiz | uspto-grants-2006_11 |