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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 722218Erstellt: 25. Oktober 2026

Cyanogen Bromide → 5-(2-Nitrophenyl)-1,3,4-oxadiazol-2-amine

https://huagongshe.com/reaction/722218

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktCyanogen BromideHCID 10476—
Edukto-NitrobenzohydrazideHCID 3781218—
LösungsmittelAcetonitrileHCID 6342—
Produkt5-(2-Nitrophenyl)-1,3,4-oxadiazol-2-amineHCID 712042—

Reaktionsschritte

4 ml of a 5M cyanogen bromide solution in acetonitrile were added dropwise to the solution of 3.6 g of 2-nitrobenzoic hydrazide in 20 ml of acetonitrile. This resulted first in a clear solution, then a solid precipitated out which was filtered off with suction after continuing to stir for a short time, washed again with acetonitrile and dried under reduced pressure.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07138414B2
Quelldatensatzuspto-grants-2006_11
ORD IDord-db67281e842a443a941f216a9cc75985
Quellennotizuspto-grants-2006_11