Morpholine → HCID 7892717, Verbindung

Reaktionsgleichung

F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][C:3]=1[C:11]([N:13]1[CH2:18][CH2:17][N:16]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH2:15][CH2:14]1)=[O:12].[NH:25]1[CH2:30][CH2:29][O:28][CH2:27][CH2:26]1>>[N:25]1([C:2]2[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][C:3]=2[C:11]([N:13]2[CH2:18][CH2:17][N:16]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH2:15][CH2:14]2)=[O:12])[CH2:30][CH2:29][O:28][CH2:27][CH2:26]1

Komponenten

Edukt 2

HCID 8083Morpholine

HCID 59793731(2-Fluoro-5-nitro-phenyl)(4-phenyl-piperazin-1-yl)-methanone

Produkt 1

HCID 7892717HCID 7892717, Verbindung

Versuchsvorschrift

The title compound was prepared according to the procedure described for example 1 from (2-Fluoro-5-nitro-phenyl)-(4-phenyl-piperazin-1-yl)-methanone and morpholine (87%, yellow solid, MS (m/e): 397.3 (M+H, 100%)

Quellen und Nachweise

ORD-Eintrag: ord-936276d58bda47388ae3ababb29c8743
Quelldatensatz: uspto-grants-2009_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07595314B2

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