Sodium borohydride → HCID 23310928, Verbindung
Reaktionsgleichung
[BH4-].[Na+].[C:3]([CH:6]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7]1([CH3:14])[CH:12]=[O:13])([CH3:5])=[CH2:4]>C(O)(C)C>[C:3]([CH:6]1[CH2:10][CH2:9][CH:8]([CH3:11])[C:7]1([CH3:14])[CH2:12][OH:13])([CH3:5])=[CH2:4]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Into a 250 ml flask equipped with stirrer, thermometer reflux condensor, heating mantle and nitrogen blanket apparatus are placed 15 grams of sodium borohydride, 100 ml anhydrous isopropyl alcohol and 65 grams of 2-isopropenyl-1,5-dimethylcyclopentane carboxaldehyde having the structure: ##STR26## prepared according to U.S. Pat. No. 4,474,992 issued on Oct. 2, 1984.
Aufarbeitung
- customInto a 250 ml flask equipped with stirrer
- temperaturethermometer reflux condensor, heating mantle and nitrogen blanket apparatus
- custom##STR26## prepared
Quellen und Nachweise
- ORD-Eintrag
- ord-bb0f43f23f4b4f94ab1524f8c3e67002
- Quelldatensatz
- uspto-grants-1986_07
- Patentnummer
- US04601850
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