N,N-Dimethyl-1,3-propanediamine → HCID 22350930, Verbindung

HRID 747534Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 747534
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[NH:7][C:8](=[S:12])SCC.[CH3:13][N:14]([CH3:19])[CH2:15][CH2:16][CH2:17][NH2:18]>C(O)C>[CH3:13][N:14]([CH3:19])[CH2:15][CH2:16][CH2:17][NH:18][C:8]([NH:7][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=1)=[S:12]

Komponenten

4

Edukt 2

HCID 7993N,N-Dimethyl-1,3-propanediamineHCID 12214896Ethyl 2-Pyridyldithiocarbamate

Produkt 1

HCID 22350930HCID 22350930, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

A mixture of ethyl 2-pyridyldithiocarbamate (600 mg), 3-(dimethylamino)propylamine (0.38 ml) and ethanol (6 ml) was heated with reflux under nitrogen atmosphere. One and half hour thereafter, the reaction mixture was concentrated under reduced pressure to give the title compound (786 mg) as crude oil.

Aufarbeitung

  1. temperaturewas heated
  2. temperaturewith reflux under nitrogen atmosphere
  3. concentrationOne and half hour thereafter, the reaction mixture was concentrated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-c55300dbfc144f439c6f699b2f6b1245
Quelldatensatz
uspto-grants-2008_07
Patentnummer
US07396842B2

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