Phenoxyacetic Acid → HCID 795591, Verbindung
Reaktionsgleichung
COc1ccc(N)cc1OC.O=C(O)COc1ccccc1.COC1=NC(=NC(=N1)Cl)Cl.CN1CCOCC1.CN(C)C=O>>COc1ccc(NC(=O)COc2ccccc2)cc1OCKomponenten
6
Reaktionsbedingungen
- Temperatur
- 25 °C
Aufarbeitung
- addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
- addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
- aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
- addition380 uL MeCN solvent were added to the transfer plate
- aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
- addition180 uL MeCN added to filter plate 1 for LCMS analysis
- aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
- addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
- customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM
Quellen und Nachweise
- ORD-Eintrag
- ord-d7534c28d51943a1850d61e7d4d62aa0
- Quelldatensatz
- AIChemEco amide coupling conditions 47k dataset
Notizen zur Reaktion
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